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DKL Engineering, Inc.
Handbook of Sulphuric Acid Manufacturing
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Contents
Acid Plant Database September 8, 2012
Owner | CJSC Crimea TITAN | |||
Location |
Armyansk Northern part of Crimea peninsula near its border with Kherson region, in the narrowest part of Crimean isthmus, on the shore of Sivash lakes, which is only 7 km away from Karakinitsky gulf of the Black Sea. |
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Background | 1969 - Crimea State Industrial Union "TITAN" (CSIU "TITAN") established | |||
Website | www.titanexport.com | |||
Plant | Plant No. 1 | Plant No. 2 | Plant No. 3 | |
Coordinates* | 46° 12' 7.5" N, 33° 39' 26" E | 46° 12' 6" N, 33° 39' 27" E | 46° 12' 7" N, 33° 39' 31" E | |
Type of Plant | Sulphur Burning | Sulphur Burning | Sulphur Burning | |
Gas Source | Elemental Sulphur - Bulk | Elemental Sulphur - Bulk | Elemental Sulphur - Bulk | |
Plant Capacity | 180,000 MTPA | 180,000 MTPA | 180,000 MTPA | |
SA/DA | - | - | - | |
Status | - | - | - | |
Year Built | - | - | - | |
Technology | - | - | - | |
Contractor | - | - | - | |
Remarks | - | - | - | |
Plant | Plant No. 4 | - | - | |
Coordinates* | - | - | - | |
Type of Plant | Sulphur Burning | - | - | |
Gas Source | Elemental Sulphur - Bulk | - | - | |
Plant Capacity | 600,000 MTPA | - | - | |
SA/DA | - | - | - | |
Status | - | - | - | |
Year Built | - | - | - | |
Technology | - | - | - | |
Contractor | - | - | - | |
Remarks | - | - | - | |
Pictures | ||||
General | - | |||
References | - | |||
News |
December 20, 2011 - Crimea TITAN
sees the construction of the new sulphuric acid production plant where
double contact/double absorption process is used nearing its completion. The
plant has a capacity of 1818.2 tonnes of finished product per 24 hours and
is a unique and the only project of its kind in Ukraine.
Pros of the future plant – increase in sulphuric acid production,
reduction of harmful emissions into environment, steam and power savings and
potentially boosting production capacity of the main product.
As of now, main
construction and installation works have been completed; technological stage
of the project has been started. Administration facilities have been set
ready to welcome the work. All units of the new plant are now seeing the
works on heat insulation, piping (6 km in total) and adjusting the equipment
being made. Installation of equipment in chemical treatment unit has been
finished and testing and run-in of this equipment is planned to start in
January, 2012. Hydraulic testing on the plant flyovers has been made,
pressure has been tested and now heat-insulation of the pipes has been
started. Installation of all
metal constructions and the main equipment in the melting compartment has
been made; “pipe-in-pipe” feed system installation works are continuing;
drying and absorption units have seen completion of brick lining in all of
the three absorbers, their packing is continuing now.
Gas channels, steam and moisture collector systems are 80% ready.
Turbine building and the main building of the plant see turbine installation
and piping works continuing. Cooler installation is nearing the end, with a
lining works planned for it further, commissioning of this facility is
scheduled to start in the January in the next year.
Increasing pump station have all pumps installed, interior finish of
the building itself finished, piping ready, electrical cabling being made
and ventilation system being tested.
Improvement of the construction site itself, concreting roadways and
pathways, improvement of overall appearance of the site suggests the
completion of the construction works is approaching.
General commissioning of the plant is scheduled to start at the end
of the February. Installation works on the site are estimated to have been
80% completed.
August 8, 2011 - Crimea Titan PJSC continues the
construction of a new sulfuric acid plant. Thus, as Deputy Technical
Director for Construction Vladimir Zayats says actually all large objects
have been already installed and there is active preparing for gas ducts and
piping installation. “In the future drying and absorption department the
installation of 60 meters high flue gas duct is completed, also there made
the acid-proof brick inner lining of three absorbers installed before - says
V. Zayats. - At the final stage finishing in the administrative building, we
are preparing for the installation of major equipment of blower. In
addition, now we are testing the bowls of future cooling towers and
finishing mounting of the frame in water treatment department."
The cooling tower itself, as well as
water treatment equipment, as Vladimir Zayats says, should be sent to the
company by the end of October. The installation of underground utilities of
shop collector has been already completed, and behind the old warehouse a
sulfur melting department is under construction. As Deputy Technical
Director for Construction Vladimir Zayats says the crews are working almost
three shifts seven days a week, and in general, their work can be estimated
on "four". "Like in any construction project there are, of course, some
difficulties, but we solve them quickly. In general, we are not lagging
behind the schedule and plan to complete the work at the specified time, -
assures Vladimir Zayats. – It is hard to specify the percentage of readiness
of the shop for commissioning, but to determine the readiness of individual
objects is quite real. Thus, the administrative building is ready for 90%,
air blast is 50% ready, drying and absorption department is to be brought
forward up to 100% completion by November 1. Department of burning and
conversion is 50% complete (only gas ducts and piping installation should be
done there). The turbine building is about 30% complete, the melting
department is 50% complete, and water treatment department is ready for 70%.
Two pumping stations are complete by 70%.
The construction of new complex for sulfuric acid production by
method of double contact and double absorption (DC / DA), capacity 1818.2
tons of finished product per day has begun September, 1 2008.
The project is unique in Eastern
Europe. Commissioning of the new plant will provide an opportunity to
increase significantly the share of sulfuric acid production, and innovative
technology will bring the rate of expenditure of energy and raw materials to
the world's industry leaders.
July 7, 2011 - New sulfuric acid plant construction at one
of the largest Ukrainian chemical enterprises – Crimea Titan PJSC – comes to
its active final stage. At the
moment, the installation of large equipment is already fully completed,
construction works started in the department of melting and preparation of
sulfur, construction of buildings for future cooling towers is completed (at
the next stage cooling unit itself will be mounted), pipelining for
communication system underground network is made and quality of works
performed is being tested. The finishing work on the administrative building
is in full swing, the fine finish of premises is started and central control
for process will eventually be posted here. Also construction works are
intensified in absorption department, turbine department, 60 meters high
flue gas duct is mounted. In general, a half of total planned volume of work
has been made. Today the construction site employs about 260 people, and by
August the number of expert personnel will increase to 450 people.
Commissioning work is scheduled to begin in Q1 2012.
March 2010
– The
plant received large-sized equipment for the new sulfuric acid production
plant - intermediate absorber (the diameter of the apparatus - 6.5 meters,
the height - 12 m).
September 12, 2008 - In the year 2005 the «OstChem Holding
AG» company set up the construction of a new modern sulfuric acid production
plant. For the years 2006-2007, the experts of the company made a thorough
feasibility study on the project, specified optimal technical points, and
chose necessary equipment.
Taking into account a considerable project cost, the company management have
made a decision to attract credit funds in addition to the ownership
capital. With this end in view, this year in July in Germany an official
meeting was held between the CJSC «Crimea TITAN» management with the
representatives of the «Ostchem Germany GmbH» company, of the one part, and
the «Commerzbank AG» firm, of the other part. In the course of the visit a
new credit agreement with the «Commerzbank AG», a contract with the prime
contractor «Chemieanlagenbau Chemnitz GmbH» and a contract with the
insurance company «Euler HERMES» have been signed.
Scheduled costs for construction of
new sulfuric acid production workshop amount to about 55 million, 25 million
of the sum is money of shareholder «OstChem Germany GmbH», and 30 million is
the credit granted by German «Commerzbank AG».
The general contractor
«Chemieanlagenbau Chemnitz GmbH» has concluded purchase contracts with
producers to buy the whole complex of thermotechnical facilities for new
workshop. The supplies according to the above contracts are planned for
April 2009. Since the 1st of
September of this year Crimea TITAN has already begun the preliminary works
for construction of new sulfuric acid production workshop (pile layout for
pointing the axes of future foundation, altimetric survey and marking up
coordinates of the main facilities on the plot plan).
Economic potential of commissioning
of up-to-date sulfuric acid production lies in cost reduction, and also
increase of production output of titanium dioxide and monoammonium phosphate
produced by Crimea TITAN. In social sphere it means new jobs for people who
live in the region. In environment protection field it means usage of new
environment safety technology in production process that will allow
minimizing the environmental impact of chemical manufacturing processes.
November 2005 - Company defined the winner of the tender on
construction of a new hi-tech shop on manufacture of a sulfuric acid by
capacity of 600 thousand t/year.
The winner of the tender become a Ukrainian-German consortium of JSL
"Cityterm" – Hugo Petersen GmbH - Chemieanlagenbau Chemnitz GmbH.
The advanced technologies and last
scientific achievements in the field of construction of chemical
installations were put in a basis of the offers of the consortium.
Prospective term of implementation of
the project - 24 months. The cost of
the project is estimated in 55 million euro.
Hugo Petersen GmbH includes following tasks: scientific
substantiation, engineering of the project and transfer of license
technology to Joint-Stock Company « Crimean Titan ».
Harmonization of the German project
will lie on shoulders of Ukrainian company "Cityterm" with the Ukrainian
norms, and also necessary expert coordination, functions general contractor
and construction on "a turn-key basis". |
MTPD - Metric Tonne per Day
STPD - Short Ton per Day
MTPA - Metric Tonne per Annum STPA - Short Ton per
Annum
SA - Single Absorption
DA - Double Absorption
* Coordinates can be used to
locate plant on Google Earth