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Sulphuric Acid on the WebTM Technical Manual DKL Engineering, Inc.

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Sulphuric Acid on the Web

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Handbook of Sulphuric Acid Manufacturing
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Sulphuric Acid Decolourization
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Process Engineering Data Sheets - PEDS
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Introduction

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Preface
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Sulphuric Acid Plant Specifications
 

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Strong Acid System - Acid Distributors - Trough Type Distributors
January 10, 2011

Trough Type Distributors

The original trough type distributors were fabricated from cast iron with a heavy wall rectangular trough.  Notches at the top edge allowed the acid to overflow into downcomers also made of cast iron.  The downcomers clipped onto the top edge of the trough and directed the acid to a point in the packing.  A feed pipe system is required to distribute the acid between the troughs.  Orifice plates installed in the feed pipe system ensure even distribution between the troughs.  Due to the size of the cast parts, cast iron distributors were only able to achieved about 15 distribution points/m² (1.4 points/ft²). sa_distcitrough.JPG (14988 bytes)
Cast iron distributors served the industry well for many years but they were not without problems and limitations.  Like all trough type distributors the trough must be absolutely level in order to achieve uniform distribution across the trough.  The ends of the troughs rested on brick corbels and brick shims were required to level the troughs.  Intermediate overhead supports were sometimes required for the longer troughs.  Uniform acid distribution in the feed pipe system is also required but this would be affected by the uneven corrosion of the orifice plates used to distribute the flow.  The troughs would often fill with sulphate and would require periodic cleaning with was both messy and dangerous.  Although the life of a cast iron distributor was acceptable, the material did corrode which meant it would eventually need to be replaced. castirondist.JPG (26566 bytes)
 

The modern trough type acid distributor is best represented by Monsanto Enviro-Chem's trough distributor.  The material of construction is a high silicon containing stainless steel which is virtually corrosion resistant.  Like the cast iron distributors, a feed pipe system is required to distribute the acid amongst the troughs but instead of cast iron, stainless steels is used.  Instead of cast iron downcomers, tubing with an oval slot near the top of the tube is used to distribute the acid from the trough to the top of the packing.

The troughs must still be installed absolutely level and distribution into the feed pipe system must be uniform for the distributor to function properly.

A distributor of this design can achieve about 43 distribution points/m² (4 points/ft²) nearly 3 times the number of the cast iron distributor.

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Distribution

One of the key objectives of the acid distributor is to achieve an even distribution of acid across the packing.  An indication of even distribution in a trough distributor is the level in troughs.  If each trough has the same operating level, even distribution can be assured.  Dipping the acid level in each trough is a good way to measure the level in each trough.  Safety precautions must be taken when dipping the troughs since it can only be done when acid is circulating over the tower.   An example of the results of dipping the troughs is shown.

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