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DKL Engineering, Inc.
Handbook of Sulphuric Acid Manufacturing
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Analytical Procedures - Moisture in Gas
Exit Drying Tower
February 24, 2002
Introduction Equipment Reagents Procedure |
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Moisture determination is performed on the drying tower outlet gas in order to check the drying efficiency of the tower itself. In fact the presence of high quantity of water in the inlet gas to the converter, can be dangerous for the catalyst.
Moisture determination is carried out, in a fast and appropriate manner, making use of commercial selective glass vial, containing a special substance that changes its colour in presence of water.
This is a fast
and easy way to perform this determination because the glass phial is already
pre calibrated, directly, in mg of water absorbed.
Supplier
Dräger Sicherheitstechnik GmbH
Part No.
6728531
Range of
Measurement
Test Volume
2 to 80 mg/m³
100 L
5 to 250 mg/m³
50 L
10 to 450 mg/m³
25 L
40 to 1600 mg/m³
10 L
Fit about 1 meter
rubber hose in a sampling probe, close the end with an Hoffman clamp. Set the
probe into the sampling point and slowly open the clamp to purge for about 30
minutes with a flow rate of approximately 60 l/m (avoiding overheating of the
rubber tube). Now insert the sample tube into the end of the rubber hose and
make a sampling operation, during a period of time long enough to colour the
vial.
The range of
measurement and accuracy can be varied depending on the size of sample taken.
Refer to the information supplied with the Dräger tube for details.