headerdrawing1.jpg (96365 bytes)

Sulphuric Acid on the WebTM Technical Manual DKL Engineering, Inc.

Knowledge for the Sulphuric Acid Industry Line.jpg (1139 bytes)

Sulphuric Acid on the Web

Introduction
General
Equipment Suppliers
Contractor

Instrumentation
Industry News
Maintenance
Acid Traders
Organizations
Fabricators
Conferences

Used Plants
Intellectual Propoerty
Acid Plant Database
Market Information
Library

Technical Manual

Introduction
General

Definitions
Instrumentation
Plant Safety
Metallurgial Processes
Metallurgical
Sulphur Burning
Acid Regeneration
Lead Chamber
Technology
Gas Cleaning
Contact
Strong Acid
Acid Storage
Loading/Unloading

Transportation
Sulphur Systems
Liquid SO2
Boiler Feed Water
Steam Systems

Cooling Water
Effluent Treatment
Utilities
Construction
Maintenance
Inspection
Analytical Procedures
Materials of Construction
Corrosion
Properties
Vendor Data

DKL Engineering, Inc.

Handbook of Sulphuric Acid Manufacturing
Order Form
Preface
Contents
Feedback

Sulphuric Acid Decolourization
Order Form
Preface
Table of Contents

Process Engineering Data Sheets - PEDS
Order Form
Table of Contents

Introduction

Bibliography of Sulphuric Acid Technology
Order Form

Preface
Contents

Sulphuric Acid Plant Specifications
 

Google Search new2.gif (111 bytes)

 

log 2.JPG (76785 bytes)

Sharplex.jpg (28953 bytes)

MAHLEInd.jpg (21078 bytes)

 


Strong Acid System - Drying Systems
September 30, 2002

Introduction

Associated Links

Acid Pump Tanks
Acid Distributors
Mist Eliminators
Acid Pumps
Acid Coolers
Acid Piping
Instrumentation and Controls


Introduction

The Drying Acid System absorbs the water vapor remaining in the gas after it leaves the Gas Cleaning Section of the plant.  The primary reason for drying the gas is to avoid corrosion caused by wet SO2 gas before the converter and by wet SO3 after conversion and to avoid acid condensation during shut-downs and thus protect the catalyst from degradation.   Drying the gas will also help to maintain a clear stack by avoiding the formation of excessive amounts of sub-micron mist particles that may over load the mist eliminators in the Final Tower.drytower.GIF (13177 bytes)

A typical Drying Acid System consists of the following items of equipment:

a)        Drying Tower

A typical Drying Tower is a vertical cyclindrical vessel designed to contact process gas and strong sulphuric acid (93 to 98.5% H2SO4) for the purpose of drying the gas.  The tower may be constructed of specialty alloys such as the high silicon stainless steels, nickel-chromium alloys or the more traditional brick lined carbon steel.  The tower will be equipped with a packing support, packing, acid distributor, and mist eliminator.

b)        Acid Pump Tank

A pump tank is required to hold the acid that is circulated in the drying acid system.  The pump tank may be constructed of specialty alloys or the more traditional brick lined carbon steel.  The pump tank holds sufficient acid to enable the circulating pumps to operate and provides sufficient room to hold the acid that drains down out of the system when the circulation is shutdown.  In some designs the pump tank is a standalone vessel or can be partially or fully integrated with the Drying Tower as is the case in a pump boot arrangement.

c)       Acid Pump

An acid pump is required to circulate the acid from the pump tank up to the distributor inside the Drying Tower.  The acid flows by gravity over the packing and drain out the bottom or side of the Drying Tower back to the pump tank.  The pump can be a vertical submerged centrifugal pump in which case it would be mounted in the pump tank.  External vertical centrifugal pumps are also available as well as horizontal centrifugal pump types, although the latter is uncommon.

d)        Acid Cooler

The absorption of water into sulphuric acid is an exothermic reaction and will cause the temperature of the acid to rise unless the heat of absorption is removed.  The heat is typically removed in either a plate heat exchanger or anodically protected shell and tube heat exchanger.

e)       Piping

Acid piping is required to carry the acid from one piece of equipment to the next.  Materials vary considerably depending on the acid concentration, temperature and cost.

f)        Instrumentation and Controls

Instrumentation and controls are required to monitor the operation of the system and control its operating parameters.  Acid concentration, flow and temperature are the most important factors in ensuring the system is performing its function of gas drying as efficiently as possible.